1232745

Etude de l’interface oxyde-solution par relaxométrie
RMN Application à la synthèse de nanoparticules
catalytiques
Pierre Flauder
To cite this version:
Pierre Flauder. Etude de l’interface oxyde-solution par relaxométrie RMN Application à la synthèse
de nanoparticules catalytiques. Physique [physics]. Ecole normale supérieure de lyon - ENS LYON,
2007. Français. �tel-00167868�
HAL Id: tel-00167868
https://tel.archives-ouvertes.fr/tel-00167868
Submitted on 23 Aug 2007
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NM
40
12
Fitting with formula: y = a0+a1*exp(-x/a2)+a3*exp(-x/a4)+a5*exp(-x/a6)
Computed values:
a0 = 0.0841248
a1 = 7.57693
a2 = 0.0459661
a3 = 33.0803
a4 = 0.00954347
a5 = 12.6358
a6 = 0.219321
Chi-square: 68.7241
Correlation coefficient: 0.999360
30
20
Fitting with formula: y = a0+a1*exp(-x/a2)+a3*exp(-x/a4)+a5*exp(-x/a6)+a7*exp(-x/a8)
Computed values:
a0 = 0.065991
a1 = 1.25199
a2 = 45.3415
a3 = 1.97153
a4 = 9.88528
a5 = 4.95572
a6 = 0.27318
a7 = 3.11226
a8 = 1.58872
Chi-square: 69.4167
Correlation coefficient: 0.993616
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Sols
Gels solides
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10000
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1 couche
adsorbee
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Amp. rel. du T2 des flocs
8
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"2*%(.'A) :*%!SC(56*m½!&2)^*6.'A*%[email protected] ;@,<"U *65m/+*6.182,<$656$6"2*%!<.D,<$6.'&2/43<.SÂ <;@&(.1^# ;@(.78:@.A',D;@& $H"2*i/4)+*%I*%!',<*m/+*6.
"2*%&ÆZ8:,3;B¿%',<*6.SÂ
QSR5TDUWVYX/Z\[]VY^ _XO_S^ T ^ `bac[Xedfghdi_]VYjha=VYXOk _b[Slm`nDac_S^ _S`VYdejhT am`mo
,6 G 3
*82_ X ( ( H ') ( WT \ ( 4 687:9 X K
* 'A ( ( > *82_ X ( ,#Rb A 2_2X ( *8W# %* ^ O'2Z'A ( O * 'A ( ( * A 8A *8 4 687:9
OH=3.405
OH=2.980
2,8
2,6
2,4
2,2
2
( ² *82_ =X ( 8#
b RCX , 4 687:9 , *:K
'A ( ( O ( # O 'AK
=c * 'A ( ( >
0
10
20
!" #$&30%'" )(*,+
40
50
3
2,8
2,6
2,4
2,2
2,5
- .0/,1 3,5
3
4
25
Fitting with formula: y = a0+a2*a1^x
a0 = 8.32126
a1 = 211536
a2 = 1.10475e-15
Chi-square: 57.751
Correlation coefficient: 0.938567
20
( D (r( ##') #( WT ( WT a *82_ YX ( K
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OH=3.4
OH=3.9
ln
r = (kd)
0.9 = 3
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r = (kd)
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ln(kd) = -17.529 + 11.503 * ln(OH)
r = 0.9956
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( ZRI 0- 2 ( - X 4 687:9>
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4
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0,44
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